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Organic synthesis is usually performed in solution to dissolve both reactants and catalysts and to deliver heat. Here, we
show that glycerol, which is a non-toxic, biodegradable, and recyclable liquid manufactured from renewable sources, has a
high potential to serve as alternative green solvent for organic reactions. Several catalytic and non-catalytic reactions
were successfully performed in glycerol. High products yields and selectivities were achieved. Besides solubility of the reactants
and the catalysts and easy separation of the product, glycerol offers several other benefits such as catalyst recycling, microwave
assisting reaction, and biphasic and emulsion modes. 相似文献
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Sotiriou M Ferguson SF Davey M Wolfson JM Demokritou P Lawrence J Sax SN Koutrakis P 《Environmental monitoring and assessment》2008,137(1-3):351-361
Particles in a dental office can be generated by a number of instruments, such as air-turbine handpieces, low-speed handpieces,
ultrasonic scalers, bicarbonate polishers, polishing cups, as well as drilling and air sprays inside the oral cavity. This
study examined the generation of particles during dental drilling and measured particle size, mass, and trace elements. The
air sampling techniques included both continuous and integrated methods. The following particle continuous measurements were
taken every minute: (1) size-selective particle number concentration (Climet); (2) total particle number concentration (PTRAK),
and; (3) particle mass concentration (DustTrak). Integrated particle samples were collected for about 5 h on each of five
sampling days, using a PM2.5 sampler (ChemComb) for elemental/organic carbon analysis, and a PM10 sampler (Harvard Impactor) for mass and elemental analyses. There was strong evidence that these procedures result in particle
concentrations above background. The dental procedures produced number concentrations of relatively small particles (<0.5 μm)
that were much higher than concentrations produced for the relatively larger particles (>0.5 μm). Also, these dental procedures
caused significant elevation above background of certain trace elements (measured by X-ray fluorescence) but did not cause
any elevation of elemental carbon (measured by thermal optical reflectance). Dental drilling procedures aerosolize saliva
and products of drilling, producing particles small enough to penetrate deep into the lungs. The potential health impacts
of the exposure of dental personnel to such particles need to be evaluated. Increased ventilation and personal breathing protection
could be used to minimize harmful effects. 相似文献
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Kristine F. Stepenuck Lois G. Wolfson Barbara W. Liukkonen Jerome M. Iles Timothy S. Grant 《Environmental monitoring and assessment》2011,174(1-4):625-633
Fecal contamination of water is a public health concern for those using the water for drinking or recreation. The EPA recommends using Escherichia coli to evaluate recreational freshwaters for fecal contamination. With limited resources available, states have recently focused on training volunteers to expand data collection and resource assessment. Several bacteria testing methods are available for use by the public; however, few studies have comprehensively evaluated their use by volunteers. This study evaluated two E. coli monitoring methods used by volunteers: Coliscan Easygel® and 3MTM PetrifilmTM, incubated for 24 and 48 hours. The methods were assessed to determine how closely each matched results with EPA-approved laboratory analyses. Analysis of covariance results indicated that when used by volunteers to monitor surface water, 3MTM PetrifilmTM results were more similar to laboratory analyses than Coliscan Easygel®. Both test methods had similar overall accuracy of predicting if a sample exceeded or fell below the 235 cfu/100 mL EPA body contact standard for recreational surface waters. Two-thirds of volunteers preferred 3MTM PetrifilmTM. 相似文献